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Beilstein J. Org. Chem. 2022, 18, 1062–1069, doi:10.3762/bjoc.18.108
Graphical Abstract
Scheme 1: Strategies for the synthesis of vic-1,2-diols.
Scheme 2: Substrate scope. Reaction conditions: 1 (1.0 mmol), Et4NBr (0.1 equiv), imidazole (0.05 equiv), MeC...
Scheme 3: Investigation of cross-coupling reaction.
Scheme 4: Large-scale experiment.
Scheme 5: Control experiments. aDetermined by 1H NMR using 1,3,5-trimethoxybenzene as an internal standard. b...
Scheme 6: Proposed mechanism.